Abstract
The high-temperature behaviour of organised mesoporous alumina was investigated using X-ray powder diffraction, nitrogen adsorption isotherms and transmission electron microscopy. Based on the combination of these methods it has been shown that organised mesoporous alumina synthesised using long-chain carboxylic acids is transformed at temperatures between 600 and 1000 °C into a material which consists of a packing of δ-alumina particles.

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