Highly concentrated omega‐3 fatty acid ethyl esters by urea complexation and molecular distillation
- 28 August 2018
- journal article
- research article
- Published by Wiley in Journal of the Science of Food and Agriculture
- Vol. 99 (2) , 877-884
Abstract
BACKGROUND: Raya liver deodorized oil contains high concentrations of eicosapentaenoic acid (EPA), docosapentaenoic acid (DPA) and docosahexaenoic acid (DHA). The present study investigated the processes of urea complexation (UC) and molecular distillation (MD) to determine the most adequate operation conditions for each process, separately and together, aiming to obtain highly concentrated EPA, DPA and DHA ethyl esters with chemical indicator values permitted by the current legislation for edible oils.RESULTS: In the second stage of MD, a concentration of 820.27 g kg−1 in the distillate and 951.06 g kg−1 of omega‐3 fatty acid ethyl esters in the residue was obtained. The distillate showed values of free fatty acids, peroxide and p‐anisidine lower than the maximum allowed for edible oils in accordance with the current legislation.CONCLUSION: The use of UC and MD together has revealed a significant improvement in the total concentration of omega‐3 fatty acid ethyl esters in the final product and good application prospects. © 2018 Society of Chemical IndustryKeywords
Funding Information
- Consejo Nacional de Investigaciones Científicas y Técnicas
- Agencia Córdoba Ciencia
This publication has 17 references indexed in Scilit:
- Concentration and purification of polyunsaturated fatty acids from squid liver processing wastesEuropean Journal of Lipid Science and Technology, 2014
- Combination of Urea Complexation and Molecular Distillation to Purify DHA and EPA from Sardine Oil Ethyl EstersJournal of the American Oil Chemists' Society, 2014
- Concentration of Omega-3 Polyunsaturated Fatty Acids from Oil of Schizochytrium limacinum by Molecular Distillation: Optimization of Technological ConditionsIndustrial & Engineering Chemistry Research, 2013
- Polyunsaturated Fatty Acid Concentrates of Carp Oil: Chemical Hydrolysis and Urea ComplexationJournal of the American Oil Chemists' Society, 2011
- Optimization of molecular distillation to concentrate ethyl esters of eicosapentaenoic (20:5 ω‐3) and docosahexaenoic acids (22:6 ω‐3) using simplified phenomenological modelingJournal of the Science of Food and Agriculture, 2011
- Monoglyceride and Diglyceride Production Through Lipase-Catalyzed Glycerolysis and Molecular DistillationApplied Biochemistry and Biotechnology, 2009
- Effect of Operating Conditions on the Concentration of Monoglycerides Using Molecular DistillationChemical Engineering Research and Design, 2007
- Concentration of docosahexaenoic acid (DHA) and eicosapentaenoic acid (EPA) of tuna oil by urea complexation: optimization of process parametersJournal of Food Engineering, 2006
- Study of purification of fatty acids, tocopherols and sterols from deodorization distillate.Grasas y Aceites, 2005
- The pseudo‐single‐phase, base‐catalyzed transmethylation of soybean oilJournal of the American Oil Chemists' Society, 2004