Two-dimensional J spectroscopy: 1H n.m.r. spectra of mono- and di-saccharides

Authors:
  • LHLaurance D. Hall
    Laurance D. Hall
  • SSSubramaniam Sukumar
    Subramaniam Sukumar
  • GSGlenn R. Sullivan
    Glenn R. Sullivan
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Abstract
1 H N.m.r. spectra (270 MHz) of trideuteriomethyl 2,3,4,6-tetrakis-O-trideuterioacetyl-α-D-glucopyranoside (1) and 2,3,4-tri-O-acetyl-6-deoxy-α-D-glycopyranosyl 3,4-di-O-acetyl-1,6-dideoxy-β-D-fructofuranoside (2) have been measured using the two-dimensional J technique; various integral projections of the complete two-dimensional spectra are presented and discussed.