Ambient pressure XPS at MAX IV
Open Access
- 24 September 2025
- journal article
- Published by Beilstein Institut in Beilstein Journal of Nanotechnology
- Vol. 16 (1) , 1677-1694
Abstract
Ambient pressure X-ray photoelectron spectroscopy (APXPS) has emerged as an important technique for investigating surface and interface chemistry under realistic conditions, overcoming the limitations of conventional XPS restricted to ultrahigh vacuum. This review highlights the capabilities and scientific impact of APXPS at the MAX IV Laboratory, the world’s first fourth-generation synchrotron light source. With the APXPS beamlines SPECIES and HIPPIE, MAX IV offers state-of-the-art instrumentation for in situ and operando studies across a broad pressure range, enabling research in catalysis, corrosion, energy storage, and thin film growth. The high brilliance and small beam size of MAX IV’s synchrotron light are essential for pushing the time-resolution boundaries of APXPS, especially in the soft X-ray regime. We discuss representative studies at MAX IV, including investigations of single-atom catalysts, confined catalysis, time-resolved catalysis, atomic layer deposition, and electrochemical interfaces, showcasing the role of APXPS in advancing material and surface science.Keywords
Funding Information
- Svenska Forskningsrådet Formas (2019-02496)
- Vetenskapsrådet (2018-07152, 2022-04363, 2017-04840)
- Crafoordska Stiftelsen
- VINNOVA (2018-04969)
This publication has 70 references indexed in Scilit:
- In depth analysis of the passive film on martensitic tool alloy: Effect of tempering temperatureCorrosion Science, 2024
- In vacuo studies on reaction mechanisms in ALD processes of ruthenium and platinum filmsApplied Surface Science, 2023
- The Oxygen Evolution Reaction Drives Passivity Breakdown for Ni–Cr–Mo AlloysAdvanced Materials, 2023
- Synchrotron-based near ambient-pressure X-ray photoelectron spectroscopy and electrochemical studies of passivation behavior of N- and V-containing martensitic stainless steelCorrosion Science, 2023
- In situ quantitative analysis of electrochemical oxide film development on metal surfaces using ambient pressure X-ray photoelectron spectroscopy: Industrial alloysApplied Surface Science, 2022
- Truth is, we all are transients: A perspective on the time-dependent nature of reactions and those who study themCatalysis Today, 2022
- Comparative study of copper oxidation protection with graphene and hexagonal boron nitrideCarbon, 2021
- Visualizing Chemical Reactions Confined under GrapheneAngewandte Chemie International Edition, 2012
- Appendix F Properties of Important Semiconductors2006
- ESCA applied to liquidsJournal of Electron Spectroscopy and Related Phenomena, 1973