Javad Gholipour

The present study focuses on advancing one of the most popular AM techniques, namely, laser powder bed fusion (LPBF) technology, which has the ability to produce complex geometry parts with minimum material waste but continues to face challenges in minimizing the surface roughness. For this purpose, a novel hybrid manufacturing technology, which applies in a single setup (in-envelope) both LPBF technology and high-speed machining, was examined in this research for the fabrication of tensile specimens with three different surface finish conditions: as-built, hybrid (in-envelope machining) and post-machining (out-of-envelope) on Inconel^® alloy 718, hereafter referred to as IN718. As the application of the IN718 alloy in service is typically specified in the precipitation-hardened condition, three different heat treatments were applied to the tensile specimens based on the most promising thermal cycles identified previously for room-temperature tensile properties by the authors. The as-built (AB) specimens had the highest average surface roughness (R_a) of 5.1 μm ± 1.6 μm, which was a significant improvement (five-fold) on the hybrid (1.0 μm ± 0.2 μm) and post-machined (0.8 μm ± 0.5 μm) surfaces. The influence of this surface roughness on the mechanical properties was studied both at ambient temperature and at 650 °C, which is close to the maximum service temperature of this alloy. Regardless of the surface conditions, the room-temperature mechanical properties of the as-fabricated IN718 specimens were within the range of properties reported for standard wrought IN718 in the annealed condition. Nonetheless, detailed examination of the strain localization behavior during tensile testing using digital image correlation showed that the IN718 specimens with AB surfaces exhibited lower ductility (global and local) relative to the hybrid and post-machined ones, most likely due to the higher surface roughness and near-surface porosity in the former. At 650 °C, even though the mechanical properties of all the heat-treated IN718 specimens surpassed the minimum specifications for the wrought precipitation-hardened IN718, the AB surface condition showed up to 4% lower strength and 33–50% lower ductility compared with the hybrid and PM surface conditions. Microfocus X-ray computed tomography (µXCT) of the fractured specimens revealed the presence of numerous open cracks on the AB surface and a predisposition for the near-surface pores to accelerate rupture, leading to premature failure at lower strains.

The present work investigates the effectiveness of two heat treatment cycles—solution treatment + aging (STA) and direct aging (DA)—on optimizing the microstructure and enhancing the mechanical properties of 18Ni-300 maraging steel (300 MS) produced by additive–subtractive hybrid manufacturing (ASHM). The STA treatment led to a fully martensitic microstructure with minor remnants of the cellular substructures associated with the solidification conditions in ASHM. DA resulted in some reverted austenite and partial dissolution of the cellular morphologies into shorter fragments. Despite the contrasting microstructures, the tensile strength and the macro- and micro-hardness were comparable between STA and DA conditions. By contrast, the potential for improving the ductility was higher with the DA heat treatment. This is attributed to the higher reverted austenite content in the samples treated by DA, i.e., up to a maximum of 13.4% compared to less than 3.0% in the STA samples. For the DA sample with the highest reverted austenite content of 13.4%, the highest local and global fracture strain values of 30.1 and 5.9 ± 0.6% were measured, while the respective values were 23.4 and 4.4 ± 0.1% for the corresponding STA sample. This work suggests that DA of 300 MS produced by ASHM is sufficient to achieve comparable hardness and tensile strength to STA, whilst maintaining reasonable ductility. Avoiding the solution treatment cycle, with its appreciably higher temperatures, could benefit the dimensional stability and surface quality that are important for ASHM of 300 MS parts.

Alloyed carbon steels used in ground engaging tools (GETs), such as shovel-teeth, can withstand high working loads, but their wear resistance is inadequate for abrasive operations in the mining industry. Different approaches to engineer protective surfaces on GETs for improving wear resistance have been developed over the years, but the effectiveness of the applied abrasive resistance layer has been limited by the maximum thickness that can be realized reliably. Considering wear requirements for GETs to reach end-of-life without requiring unscheduled maintenance for after-failure repairs, a minimum thickness of 25 mm has been postulated for the abrasive resistance surface layer, which is roughly four times greater than the thickness of overlays currently manufacturable by weld deposition technologies. Thus, in this study, a novel approach for conceiving thick abrasive surface protection layers—that are unlimited in thickness—on GETs is presented. The method involves applying solid-state linear friction welding and was demonstrated to be feasible for joining abrasive-resistant CPM 15V tool steel to an alloyed carbon steel (extracted from a shovel-tooth). After welding, the integrity of the joints was examined microscopically using optical and scanning electron microscopy to understand the microstructural characteristics, as well as through microhardness and tensile testing to evaluate the performance. A high frequency welding condition was identified that provided integral bonding (i.e., without voids and cracking) at the interface between the CPM 15V tool steel and alloyed carbon shovel-tooth steel. In the as-welded condition, the measured hardness profiles across the joints showed minor softening of both base materials in the heat-affected zone just adjacent to the weld center; this was attributed to over aging of the tempered martensite structures of CPM 15V tool steel and alloyed carbon shovel-tooth steel. The maximum tensile strength of the joint (553 MPa) provides evidence for the viability of linear friction welding technology for joining protective surface materials on GETs.

This study investigated the application of an in envelope additive/subtractive (LPBF) manufacturing method (Matsuura LUMEX-Avance-25) to fabricate IN718 benchmarking coupons. The coupons were then examined comprehensively for surface finish both with and without high-speed micro-machining. The microstructure of the manufactured IN718 coupons was investigated thoroughly in the as-fabricated condition and following three different standard and one non-standard post-processing heat treatments. As built coupons revealed columnar grain morphology mainly along the direction with a cellular dendritic sub-grain structure and without any strengthening precipitates. Grain size, aspect ratio, and texture were maintained after each of the applied four heat treatments. Only one of the standard heat treatments resulted in the δ phase formation. The other three heat treatments effectively dissolved the Laves phase preventing the δ formation while promoting the formation of γ′/γ″ precipitates. Despite the observed differences in their microstructures, all of the heat treatments resulted in similar yield and ultimate tensile strength values that ranged between 1103–1205 MPa and 1347–1387 MPa, respectively. These values are above the minimum requirements of 1034 MPa and 1241 MPa for the wrought material. The non-standard heat treatment provided the highest elongation of 24.0 ± 0.1% amongst all the heat-treated specimens without a significant loss in strength, while the standard heat treatment for the wrought parts resulted in the lowest elongation of 18.3 ± 0.7% due to the presence of δ phase.

This research study investigated the hybrid processing of 316L stainless steel using laser powder bed (LPB) processing with high-speed machining in the same build envelope. Benchmarking at four laser powers (160 W, 240 W, 320 W, and 380 W) was undertaken by building additively with machining passes integrated sequentially after every ten deposited layers, followed by the final finishing of select surfaces. The final geometry was inspected against the computer-aided design (CAD) model and showed deviations smaller than 280 µm for the as-built and machined surfaces, which demonstrate the good efficacy of hybrid processing for the net-shape manufacturing of stainless steel products. The arithmetic average roughness values for the printed surfaces, Ra (linear) and Sa (surface), were 11.4 um and 14.9 um, respectively. On the other hand, the vertical and horizontal machined surfaces had considerably lower roughness, with Ra and Sa values ranging between 0.33 µm and 0.70 µm. The 160 W coupon contained layered, interconnected lack of fusion defects which affected the density (7.84 g·cm⁻³), yield strength (494 MPa), ultimate tensile strength (604 MPa), Young’s modulus (175 GPa), and elongation at break (17.3%). By contrast, at higher laser powers, near-full density was obtained for the 240 W (7.96 g·cm⁻³), 320 W (7.94 g·cm⁻³), and 380 W (7.92 g·cm⁻³) conditions. This, combined with the isolated nature of the small pores, led to the tensile properties surpassing the requirements stipulated in ASTM F3184—16 for 316L stainless steel.

To better support the transition to more industrial uses of additive manufacturing, this study examined the use of an Arcam Q20+ industrial 3D printer for producing heavily nested Ti-6Al-4V parts with both in-specification (IS) and out of specification (OS) oxygen content in reused grade 5 powder chemistries. Both the OS and IS powder chemistries were evaluated to understand their impact on build integrity and on static and fatigue performance. The results from our evaluations showed that controlling the bed preheat temperature in the Q20+ to relatively low values (326–556 °C) was effective in limiting microstructural coarsening during the long build time and enabled adequate/balanced performance vis à vis the tensile strength and ductility. Overall, the tensile properties of the IS Ti-6Al-4V material in the as-built and machined states fully met the requirements of ASTM F2924-14. By contrast, the ductility was compromised at oxygen levels above 0.2 wt.% (OS) in Ti-6Al-4V produced by EBM. Removal of the surface layer by machining increased the consistency and performance of the IS and OS Ti-6Al-4V materials. The fatigue behaviour of the EBM Ti-6Al-4V material was in the range of properties produced by casting. Due to the strong influence of both the surface finish and oxygen content on the fatigue strength, the IS Ti-6Al-4V material exhibited the highest performance, with results that were in the range of parts that had been cast plus hot isostatically pressed.

Hybrid manufacturing is often used to describe a combination of additive and subtractive processes in the same build envelope. In this research study, hybrid manufacturing of 18Ni-300 maraging steel was investigated using a Matsuura LUMEX Avance-25 system that integrates metal additive manufacturing using laser powder bed fusion (LPBF) processing with high-speed machining. A series of benchmarking coupons were additively printed at four different power levels (160 W, 240 W, 320 W, 380 W) and with the integration of sequential machining passes after every 10 deposited layers, as well as final finishing of selected surfaces. Using non-contact three-dimensional laser scanning, inspection of the final geometry of the 18Ni-300 maraging steel coupons against the computer-aided design (CAD) model indicated the good capability of the Matsuura LUMEX Avance-25 system for net-shape manufacturing. Linear and areal roughness measurements of the surfaces showed average Ra/Sa values of 8.02–14.64 µm for the as-printed walls versus 0.32–0.80 µm for the machined walls/faces. Using Archimedes and helium (He) gas pycnometry methods, the part density was measured to be lowest for coupons produced at 160 W (relative density of 93.3–98.5%) relative to those at high power levels of 240 W to 380 W (relative density of 99.0–99.8%). This finding agreed well with the results of the porosity size distribution determined through X-ray micro-computed tomography (µCT). Evaluation of the static tensile properties indicated that the coupons manufactured at the lowest power of 160 W were ~30% lower in strength, 24% lower in stiffness, and more than 80% lower in ductility relative to higher power conditions (240 W to 380 W) due to the lower density at 160 W.

The use of joints fabricated from dissimilar titanium alloys allows the design of structures with local properties tailored to different service requirements. To develop welded structures for aerospace applications, particularly under critical loading, an understanding of the fatigue behavior is crucial, but remains limited, especially for solid-state technologies such as linear friction welding (LFW). This paper presents the fatigue behavior of dissimilar titanium alloys, Ti–6Al–4V (Ti64) and Ti–6Al–2Sn–4Zr–2Mo–0.1Si (Ti6242), joined by LFW with the aim of characterizing the stress versus number of cycles to failure (S-N) curves in both the low- and high-cycle fatigue regimes. Prior to fatigue testing, metallurgical characterization of the dissimilar alloy welds indicated softening in the heat-affected zone due to the retention of metastable β, and the typical practice of stress relief annealing (SRA) for alleviating the residual stresses was effective also in transforming the metastable β to equilibrated levels of α + β phases and recovering the hardness. Thus, the dissimilar alloy joints were fatigue-tested in the SRA (750 °C for 2 h) condition and their low- and high-cycle fatigue behaviors were compared to those of the Ti64 and Ti6242 base metals (BMs). The low-cycle fatigue (LCF) behavior of the dissimilar Ti6242–Ti64 linear friction welds was characterized by relatively high maximum stress values (~ 900 to 1100 MPa) and, in the high-cycle fatigue (HCF) regime, the fatigue limit of 450 MPa at 10⁷ cycles was just slightly higher than that of the Ti6242 BM (434 MPa) and the Ti64 BM (445 MPa). Fatigue failure of the dissimilar titanium alloy welds in the low-cycle and high-cycle regimes occurred, respectively, on the Ti64 and Ti6242 sides, roughly 3 ± 1 mm away from the weld center, and the transitioning was reasoned based on the microstructural characteristics of the BMs.

Solid-state welding offers distinct advantages for joining reactive materials, such as magnesium (Mg) and its alloys. This study investigates the effect of linear friction welding (LFW) on the microstructure and mechanical properties of cast AZ91 (Mg–9Al–1Zn) and AZ91–2Ca alloys, which (to the best knowledge of the authors) has not been reported in the literature. Using the same set of LFW process parameters, similar alloy joints—namely, AZ91/AZ91 and AZ91–2Ca/AZ91–2Ca—were manufactured and found to exhibit integral bonding at the interface without defects, such as porosity, inclusions, and/or cracking. Microstructural examination of the AZ91/AZ91 joint revealed dissolution of the Al-rich second phase in the weld zone, while the Mn containing phases remained and were refined. In the AZ91–2Ca/AZ91–2Ca joint, the weld zone retained Ca- and Mn-rich phases, which were also refined due to the LFW process. In both joint types, extensive recrystallization occurred during LFW, as evidenced by the refinement of the grains from ~1000 µm in the base materials to roughly 2–6 µm in the weld zone. These microstructural changes in the AZ91/AZ91 and AZ91–2Ca/AZ91–2Ca joints increased the hardness in the weld zone by 32%. The use of digital image correlation for strain mapping along the sample gage length during tensile testing revealed that the local strains were about 50% lower in the weld zone relative to the AZ91 and AZ91–2Ca base materials. This points to the higher strength of the weld zone in the AZ91/AZ91 and AZ91–2Ca/AZ91–2Ca joints due to the fine grain size, second phase refinement, and strong basal texture. Final fracture during tensile loading of both joints occurred in the base materials.

The primary objective of this research was to develop a finite element model specifically designed for electron beam additive manufacturing (EBAM) of Ti-6Al-4V to understand metallurgical and mechanical aspects of the process. Multiple single-layer and 10-layer build Ti-6Al-4V samples were fabricated to validate the simulation results and ensure the reliability of the developed model. Thin wall plates of 3 mm thickness were used as substrates. Thermocouple measurements were recorded to validate the simulated thermal cycles. Predicted and measured temperatures, residual stresses, and distortion profiles showed that the model is quite reliable. The thermal predictions of the model, when validated experimentally, gave a low average error of 3.7%. The model proved to be extremely successful for predicting the cooling rates, grain morphology, and the microstructure. The maximum deviations observed in the mechanical predictions of the model were as low as 100 MPa in residual stresses and 0.05 mm in distortion. Tensile residual stresses were observed in the deposit and the heat-affected zone, while compressive stresses were observed in the core of the substrate. The highest tensile residual stress observed in the deposit was approximately 1.0 σ_ys (yield strength). The highest distortion on the substrate was approximately 0.2 mm.