Johan Ewald Westraadt

The effective operation of ageing coal-fired power plants requires routine damage assessment of critical component materials throughout their service history. Traditional post-exposure mechanical testing typically requires large amounts of material for each testing condition. This study introduces an accelerated (high stress and temperature) creep testing technique that employs digital image correlation for strain measurement over a non-uniform temperature field generated by a thermomechanical tester. When applied to different ex-service (exposed to service conditions within a power plant) 12% Cr piping steels, multiple accelerated creep curves at temperatures ranging from 550°C to 600°C are measured from a single specimen for each material condition. Higher creep damage in the steel due to longer service exposure and higher void densities is revealed by shorter rupture times, faster creep rates and tertiary-dominated creep curves when compared to the lower creep damage state. Microstructural study via quantitative electron microscopy confirms the dislocation creep-driven growth of subgrains in the specimen gauge regions relative to the grips. Larger subgrains and a weakening of precipitate distributions for the high damage material were also noted. Digital image correlation–measured strains are in good agreement with traditional techniques of creep testing with standard extensometry. On a comparative basis, the technique is shown to be a plausible form of damage assessment of 12% Cr piping steels with varying levels of service exposure and serve as a suitable mechanical complement to the traditional void replica methodology.

The lifetime of steam pipelines in long-term operation in coal-fired power plants are limited due to material damage that resulted from creep exposure. In the present study, the authors comparatively assess the damage of ex-service 12% Cr piping steel with varying degrees of exposure while using accelerated creep tests that employ digital image correlation (DIC) as well as microstructural investigation that is based on electron microscopy. The DIC technique, which allows multiple creep curves to be measured at temperatures ranging from 550–600 °C from a single specimen, revealed higher Zener–Hollomon parameters for a high damage material with a high void density when compared to a material with lower damage and lower void density. Both of the material states showed similar hardness values, subgrain sizes, and boundary character, despite the difference in void densities. Slightly higher inter-particle spacing of MX precipitates results in a lower threshold stress of 79 MPa for the high damage steel when compared to 97 MPa for the low damage material. Besides large Laves phase particles (>0.2 µm) that are found in the higher damaged materials that result in solid solution depletion, the most prominent microstructural damage indicator was a lower density of M₂₃C₆ precipitates. Therefore, the observations indicate that the Zener–Hollomon parameter and M₂₃C₆ particles are good damage assessment indicators between the most extreme damage states and they predict a lower damage level for a medium void density material.