Lionel Germain

Electron Backscattering Diffraction (EBSD) provides important information to discriminate phase transformation products in steels. This task is conventionally performed by an expert, who carries a high degree of subjectivity and requires time and effort. In this paper, we question if Convolutional Neural Networks (CNNs) are able to extract meaningful features from EBSD-based data in order to automatically classify the present phases within a steel microstructure. The selected case of study is ferrite-martensite discrimination and U-Net has been selected as the network architecture to work with. Pixel-wise accuracies around ~95% have been obtained when inputting raw orientation data, while ~98% has been reached with orientation-derived parameters such as Kernel Average Misorientation (KAM) or pattern quality. Compared to other available approaches in the literature for phase discrimination, the models presented here provided higher accuracies in shorter times. These promising results open a possibility to work on more complex steel microstructures.

The α and prior β textures and microtextures of a lamellar Ti6242 forged disk were characterized by advanced electron back scattered diffraction (EBSD) and related to crystallographic features of faceted crack initiation sites of dwell fatigue specimens tested along the radial direction (RD). Large feather-like structures of α colonies with close orientations were observed at boundaries of elongated prior β grains. Their orientation belongs to the α//z fiber, aligning the c-axis in RDs (z: axial direction of the disk). They are inherited from prior β grains belonging to the major β and minor β//z fibers. These feather-like structures are strong regions of the forging that act as a preferential crack initiation site. Adjacent to them, one can observe large colony with evidence of prismatic slip. Thus, the facet formation seems triggered by stress redistribution from “weak” to “strong” regions due to the elastic and plastic anisotropy. Finally, the occurrence of neighboring β grains able to share close oriented feather-like colonies is discussed considering the reconstructed β microtexture and texture. This study may be helpful for further texture control during the forging process.

The stability of lath-like microstructures during low-temperature isothermal ageing was analyzed in a Fe5Ni0.33C (in wt %) steel. The microstructures were characterized using Scanning Electron Microscopy (SEM) coupled with Electron Backscatter Diffraction (EBSD). Advanced orientation data processing was applied to quantify the hierarchical and multiscale organization of crystallographic variants subdividing Prior Austenite Grains (PAG) into packets/blocks/sub-blocks. The result shows that ferrite laths of martensite or lower bainite are stable, whatever the ageing temperature (up to 380 °C). On the contrary, a granularization process is triggered when microstructures contain a fraction of upper bainite. This metallurgical evolution corresponds to a rapid and significant change of the ferrite matrix involving a disappearance of 60° disoriented blocks. The phenomenon affects in turn the mechanical properties. The final microstructures obtained after isothermal holding look like granular bainite, which raises some questions about the classification of bainite.

The stability of lath-like microstructures during low-temperature isothermal ageing was analyzed in a Fe5Ni0.33C (in wt.%) steel. The microstructures were characterized using Scanning Electron Microscopy (SEM) coupled with Electron Backscatter Diffraction (EBSD). Advanced orientation data processing was applied to quantify the hierarchical and multiscale organization of crystallographic variants subdividing Prior Austenite Grains (PAG) into packets/blocks/sub-blocks. The result shows that ferrite laths of martensite or lower bainite are stable whatever the ageing temperatures (up to 380°C). On the contrary, a granularization process is triggered when microstructures contain a fraction of upper bainite. This metallurgical evolution corresponds to a rapid and significant change of the ferrite matrix involving a disappearance of 60° disoriented blocks. The phenomenon affects in turn the mechanical properties. The final microstructures obtained after isothermal holding look like granular bainite, which raises some questions about the classification of bainite.

Near β titanium alloys can now compete with quasi-α or α/β titanium alloys for airframe forging applications. The body-centered cubic β-phase can represent up to 40% of the volume. However, the way that its elastic anisotropy impacts the mechanical behavior remains an open question. In the present work, an advanced elasto-viscoplastic self-consistent model is used to investigate the tensile behavior at different applied strain rates of a fully β-phase Ti alloy taken as a model material. The model considers crystalline anisotropic elasticity and plasticity. It is first shown that two sets of elastic constants taken from the literature can be used to well reproduce the experimental elasto-viscoplastic transition, but lead to scattered mechanical behaviors at the grain scale. Incompatibility stresses and strains are found to increase in magnitude with the elastic anisotropy factor. The highest local stresses are obtained toward the end of the elastic regime for grains oriented with their direction parallel to the tensile axis. Finally, as a major result, it is shown that the elastic anisotropy of the β-phase can affect the distribution of slip activities. In contrast with the isotropic elastic case, it is predicted that {112} slip systems become predominant at the onset of plastic deformation when elastic anisotropy is considered in the micromechanical model.

For the β phase of Ti-5553-type metastable β-Ti alloys, striations in transmission electron microscopy (TEM) bright- and dark-field images have been frequently observed but their origin has not been sufficiently investigated. In the present work, this phenomenon is studied in depth from the macroscopic scale by neutron diffraction to the atomic scale by high-resolution TEM. The results reveal that the β phase contains homogeneously distributed modulated structures, intermediate between that of the β phase (cubic) and that of the α phase or the ω phase (hexagonal), giving rise to the appearance of additional diffraction spots at 1/2, 1/3 and 2/3 β diffraction positions. The intermediate structure between β and α is formed by the atomic displacements on each second {110}_βplane in the \langle 1{\overline 1}0\rangle_{\beta} direction, whereas that between β and ω is formed by atomic displacements on each second and third {112}_βplane in the opposite \langle 11{\overline 1}\rangle_{\beta } direction. Because of these atomic displacements, the {110}_βand {112}_βplanes become faulted, resulting in the streaking of β diffraction spots and the formation of extinction fringes in TEM bright- and dark-field images, the commonly observed striations. The present work reveals the origin of the striations and the intrinsic correlation with the additional electron reflections of the β phase.