Jane Evans

The Derbyshire Peak District in central England was one of the largest lead-producing regions in medieval Europe, yet the early history of production is obscure. Here, the authors use tooth-enamel-based lead concentrations accumulated in childhood in three cemeteries, linked to radiocarbon dates, to identify the development of post-Roman lead smelting from the mid-seventh century, with large-scale production and contamination around key mines, including Castleton, by the mid-eighth century AD. Intra- and inter-site comparisons of lead concentrations hint at the social dynamics of producer communities that may provide a benchmark for identifying lead- and silver-producing communities in medieval Europe more widely.

Though mortuary practices seem largely archaeologically invisible in Iron Age Britain, the visible dead were subject to diverse treatment. Here, the authors report the results of a multi-strand analysis of two Iron Age skeletons buried in a stone cairn at Loch Borralie, north-west Scotland. Manipulation of one skeleton, including the possible removal of the brain, fashioning of long bones into ‘tools’ and reassembly for burial, suggests complex mortuary processing, while the east-coast origin of both individuals and their biological ties to Orkney reveal long-distance connections, expanding our understanding of funerary practice, mobility and connectivity in Iron Age Britain.

Strontium isotopes ( ⁸⁷ Sr/ ⁸⁶ Sr) are increasingly used as a provenance tool in multiple disciplines. Application to biological materials requires knowledge of the variation in bioavailable ⁸⁷ Sr/ ⁸⁶ Sr across the landscape, potentially in the form of an isoscape (a quantitative model of spatial isotopic variability). This paper summarizes and provides advice on our current understanding of the main concerns in creating and interpreting isoscapes of bioavailable ⁸⁷ Sr/ ⁸⁶ Sr. Isoscape creation approaches include domain mapping, geostatistical contour mapping and machine learning, the last becoming more readily achievable with the availability of software packages. It is critically important to develop isoscapes at a resolution appropriate for addressing the research questions. Choice of sample materials depends on the research questions and availability: plants or fauna with small ranges are favoured, with some analytes (snails, soil leachates) posing challenges. Interpreting ⁸⁷ Sr/ ⁸⁶ Sr in biological tissues requires considering Sr metabolism and the timing of tissue formation, thus far underappreciated. The numerous sources of error involved in developing and applying isoscapes must be recognized to avoid over-interpreting data and spurious provenance precision. We hope this paper will help researchers investigating provenance, mobility, landscape use and migration to develop the most appropriate isoscapes for their purposes, and possible future use by others.

The stable isotopes of sulfur provide a distinctive signature for marine proximity and interaction. Exploring coastal proximity has been the principal application of sulfur isotopes in archaeology and palaeoecology, but this deals only with high (greater than 14‰) isotope values, meaning little interpretation has been gained from lower values. Progress has been hindered by issues with biosphere mapping. Air pollution can impact modern landscapes, significantly lowering sulfur isotope baselines, leading to the assumption that modern vegetation-based sulfur maps are not reliable. This research explores the potential of previously undiagnostic low, and often, negative sulfur isotope values for identifying wetland dwellers. Impervious clays that support wetlands are distinctive ecosystems and this study tests the hypothesis that they will produce low isotope values owing to both the underlying substrate and to redox conditions. Primary mapping of targeted areas using modern plants highlights zones with natural negative sulfur values and demonstrates that this constitutes a distinctive wetland signature. Analysis of modern and archaeological fauna demonstrates that these distinctive isotope compositions are transferred into the food chain. These findings propel the interpretative potential of sulfur isotopes forward and add to the growing knowledge to provide means for identifying archaeological humans and animals raised in wetlands.

Lead (Pb) isotopes provide a complementary method to other provenance tools for tracking the origin and movement of humans and animals. The method is founded in the geographic distribution of Pb isotope ratios. However, unlike the Sr isotope method that is closely linked to the lithology of underlying rocks, Pb more closely reflects the tectonic regimes. This makes it particularly pertinent to use in Britain as there is major tectonic boundary (the Iapetus Suture) that runs between Berwick-upon-Tweed and the Solway Firth providing a compositional boundary in Pb isotope domains that approximates to the geographic areas of Scotland versus England and Wales. Modern pollution makes it difficult to use modern floral or faunal samples to characterize biosphere variation, and so we use geological datasets to define isoscape variation and present the first Pb isotope map of Britain. We have validated the use of these data form biosphere studies using well provenanced samples. Reference fields of diagnostic compositions, are created in μ-T space and these have been used in a test case to assess the geographic origins of Neolithic animals in Great Britain.

Within post‐conflict communities, attempts to identify and repatriate unidentified and missing individuals poses a difficult task. As current forensic strategies commonly lack the capacity to provide region of origin assessments, forensic anthropologists/investigators are often unable to identify sources of DNA for kinship analysis. Using Thermal Ionization Mass Spectrometry (TIMS), hair samples from 10 volunteers were used to assess the variation in strontium isotope ratios (⁸⁷Sr/⁸⁶Sr) between extant people in Guatemala City and Coban; with a leach (external) and digest (dietary) signal analyzed for each sample. A two‐way anova demonstrated that the difference between ⁸⁷Sr/⁸⁶Sr of Guatemala City and Coban was statistically significant (F [1, 16] = 259.839, p < 0.05), with no statistically significant differences observed between leach and digest ⁸⁷Sr/⁸⁶Sr (F [1,16] = 4.319, p = 0.054). Overall, individuals from Coban demonstrate ⁸⁷Sr/⁸⁶Sr comparable to previously recorded baseline values, demonstrating a minimal change in diet which is reflected in associated surveys. Volunteers from Guatemala City, however, show a marked shift in ⁸⁷Sr/⁸⁶Sr away from predicted values highlighting the potential influence of imported goods. The results here highlight the applicability of ⁸⁷Sr/⁸⁶Sr in hair to serve as a potential tool to support the identification of unknown individuals in Guatemala in a forensic context.

This study utilises multi-isotope approaches to investigate early medieval diet and childhood origins of individuals interred in an unusual group burial from Lothian, Scotland. In 1976, the skeletal remains of nine adults and five infants were unearthed from the infill of a latrine of a bathhouse at the Roman fort at Cramond, Edinburgh. Originally thought to be later medieval (14^th/15^thcentury), but recently dated to the 6^thcentury AD, these remains represent a rare opportunity to gain deeper insights into the dietary histories and lifetime mobility of the inhabitants of early medieval south-central Scotland. Bone and teeth from the adults (n=9) were sampled, along with local faunal bone from a range of species (n=12). Long-term dietary trends were explored using stable carbon (δ¹³C), nitrogen (δ¹⁵N) and sulphur (δ³⁴S) isotope analyses of bone collagen, focusing on inter-individual variability and the potential inclusion of marine protein in the diet. Sulphur (δ³⁴S) was also utilised as a possible indicator of later-life mobility. Strontium (⁸⁷Sr/⁸⁶Sr) and oxygen (δ¹⁸O_CARB) ratios of tooth enamel were employed to identify potential locals and non-locals, as well as possible locations of childhood origin. No intra-group dietary variability was detected, and the results are similar to other contemporary populations from southern Britain. The sulphur isotope data indicate that all of the individuals likely lived locally in their last few decades of life. However, based on isotopic data from tooth enamel, at least one or perhaps two of the individuals likely spent their childhoods in other locations.